Indian Journal of Advances in Chemical Science, Volume: 9, Issue :2, April 2021

 
             
   
   

ISSN No.: 2320-0898 (Print); 2320-0928 (Electronic)

DOI: 10.22607/IJACS.2021.902002

   

Research Article

 

     

A Rapid and Reproducible Near Infrared Spectroscopy based Method for
Solvency Power Measurement of Dearomatized Solvents

   
Dharmendra Pandey*, Shalini Gupta, Bharat Newalkar
 

ABSTRACT

 

Today, dearomatized hydrocarbon solvents are widely used in manufacturing, cosmetic, and fast moving consumer goods sectors due to onset of stringent environmental norms. Conventionally, the solvency of such solvents is measured in terms of Kauri Butanol (KB) value. The measurement of KB value, as per ASTM-D1133, is costly, time consuming, and tedious process. To overcome such limitations, the present study reports, an innovative method using Fourier Transform-Near Infra-Red (FT-NIR) spectroscopy based rapid and reliable technique for estimation of solvency power. Partial least squares regression was used to develop calibration and prediction of KB value by the use of TQ Analyst 8 software associated with FT-NIR analyzer. This method is fast, safe, reliable, nondestructive, and inexpensive contrary to conventional procedures. The results obtained based on developed method are found to be in good agreement with those reported based on standard test method, that is, ASTM-D1133.

     
     

Key words: Kauri Butanol value, Solvency power, Fourier transform-near infra-red spectroscopy.

 

 

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